Eco-friendly, Facile and Rapid Way for Synthesis of Selenium Nanoparticles Production, structural and morphological characterisation

Cavalu, Simona; Kamel, Earar; Laslo, Vasile; Fritea, Luminita; Costea, Traian; Antoniac, Iulian Vasile; Vasile, Eugeniu; Antoniac, Aurora; Semenescu, Augustin; Mohan, Aurel; Saceleanu, Vicentiu; Vicas, Simona

Simona Cavalu, Earar Kamel, Vasile Laslo, Luminita Fritea, Traian Costea, Iulian Vasile Antoniac, Eugeniu Vasile, Aurora Antoniac, Augustin Semenescu, Aurel Mohan, Vicentiu Saceleanu, Simona Vicas

Eco-friendly, Facile and Rapid Way for Synthesis of Selenium Nanoparticles Production, structural and morphological characterisation

Abstract:

A green chemistry approach to synthesize biocompatible selenium nanoparticles is proposed in this work, using hydrogen selenite (NaHSeO3) as selenium precursor and lactose as reducing agent. The formation of nanoparticles was confirmed by dynamic light Scattering, revealing a gaussian size distribution, the maximum percentage being in the range of 20-40 nm. Zeta potential measurement indicates a negative charge -38.2 mV, the stability of selenium colloidal sol being also confirmed by UV-visible spectroscopy. TEM and AFM revealed the homogeneous, spherical shape, confirming the size of nanoparticles in the range of 20-40 nm. Structural investigations of powder selenium nanoparticles by FTIR spectroscopy and XRD patterns emphasise the presence of stretching and bending vibrations of Se-O bonds, respectively the amorphous structure of the synthesized selenium. The proposed method is suitable for biological applications such drug release, functional food or nutritional supplements.

Keywords:
selenium nanoparticles; lactose; morphology; TEM; DLS; AFM

Issue: 2017, Volume 68, Issue 12

Pages: 2963-2966

Publication date: 2018/1/15

https://doi.org/10.37358/RC.17.12.6017

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This article is published under the Creative Commons Attribution 4.0 International License

Citation Styles

Cite this article as:
CAVALU, S., KAMEL, E., LASLO, V., FRITEA, L., COSTEA, T., ANTONIAC, I.V., VASILE, E., ANTONIAC, A., SEMENESCU, A., MOHAN, A., SACELEANU, V., VICAS, S., Eco-friendly, Facile and Rapid Way for Synthesis of Selenium Nanoparticles Production, structural and morphological characterisation, Rev. Chim., 68(12), 2017, 2963-2966.

Vancouver
Cavalu S, Kamel E, Laslo V, Fritea L, Costea T, Antoniac IV, Vasile E, Antoniac A, Semenescu A, Mohan A, Saceleanu V, Vicas S. Eco-friendly, Facile and Rapid Way for Synthesis of Selenium Nanoparticles Production, structural and morphological characterisation. Rev. Chim.[internet]. 2017 Dec;68(12):2963-2966. Available from: https://doi.org/10.37358/RC.17.12.6017

APA 6th edition
Cavalu, S., Kamel, E., Laslo, V., Fritea, L., Costea, T., Antoniac, I.V.,... Vicas, S. (2017). Eco-friendly, Facile and Rapid Way for Synthesis of Selenium Nanoparticles Production, structural and morphological characterisation. Revista de Chimie, 68(12), 2963-2966. https://doi.org/10.37358/RC.17.12.6017

Harvard
Cavalu, S., Kamel, E., Laslo, V., Fritea, L., Costea, T., Antoniac, I.V., Vasile, E., Antoniac, A., Semenescu, A., Mohan, A., Saceleanu, V., Vicas, S. (2017). 'Eco-friendly, Facile and Rapid Way for Synthesis of Selenium Nanoparticles Production, structural and morphological characterisation', Revista de Chimie, 68(12), pp. 2963-2966. https://doi.org/10.37358/RC.17.12.6017

IEEE
S. Cavalu, E. Kamel, V. Laslo, L. Fritea, T. Costea, I.V. Antoniac, E. Vasile, A. Antoniac, A. Semenescu, A. Mohan, V. Saceleanu, S. Vicas, "Eco-friendly, Facile and Rapid Way for Synthesis of Selenium Nanoparticles Production, structural and morphological characterisation". Revista de Chimie, vol. 68, no. 12, pp. 2963-2966, 2017. [online]. https://doi.org/10.37358/RC.17.12.6017

Text
Simona Cavalu, Earar Kamel, Vasile Laslo, Luminita Fritea, Traian Costea, Iulian Vasile Antoniac, Eugeniu Vasile, Aurora Antoniac, Augustin Semenescu, Aurel Mohan, Vicentiu Saceleanu, Simona Vicas,
Eco-friendly, Facile and Rapid Way for Synthesis of Selenium Nanoparticles Production, structural and morphological characterisation,
Revista de Chimie,
Volume 68, Issue 12,
2017,
Pages 2963-2966,
ISSN 2668-8212,
https://doi.org/10.37358/RC.17.12.6017.
(https://revistadechimie.ro/Articles.asp?ID=6017)
Keywords: selenium nanoparticles; lactose; morphology; TEM; DLS; AFM

RIS
TY - JOUR
T1 - Eco-friendly, Facile and Rapid Way for Synthesis of Selenium Nanoparticles Production, structural and morphological characterisation
A1 - Cavalu, Simona
A2 - Kamel, Earar
A3 - Laslo, Vasile
A4 - Fritea, Luminita
A5 - Costea, Traian
A6 - Antoniac, Iulian Vasile
A7 - Vasile, Eugeniu
A8 - Antoniac, Aurora
A9 - Semenescu, Augustin
A10 - Mohan, Aurel
A11 - Saceleanu, Vicentiu
A12 - Vicas, Simona
JF - Revista de Chimie
JO - Rev. Chim.
PB - Revista de Chimie SRL
SN - 2668-8212
Y1 - 2017
VL - 68
IS - 12
SP - 2963
EP - 2966
UR - https://doi.org/10.37358/RC.17.12.6017
KW - selenium nanoparticles
KW - lactose
KW - morphology
KW - TEM
KW - DLS
KW - AFM
ER -

BibTex
@article{RevCh2017P2963,
author = {Cavalu Simona and Kamel Earar and Laslo Vasile and Fritea Luminita and Costea Traian and Antoniac Iulian Vasile and Vasile Eugeniu and Antoniac Aurora and Semenescu Augustin and Mohan Aurel and Saceleanu Vicentiu and Vicas Simona},
title = {Eco-friendly, Facile and Rapid Way for Synthesis of Selenium Nanoparticles Production, structural and morphological characterisation},
journal = {Revista de Chimie},
volume = {68},
number = {12},
pages = {2963-2966},
year = {2017},
issn = {2668-8212},
doi = {https://doi.org/10.37358/RC.17.12.6017},
url = {https://revistadechimie.ro/Articles.asp?ID=6017}
}

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