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https://doi.org/10.37358/Rev.Chim.1949

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ISSN Online 2668-8212
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Revista de Chimie (Rev. Chim.), Year 2017, Volume 68, Issue 4, 639-641

https://doi.org/10.37358/RC.17.4.5521

Adina Ionuta Gavrila, Ioana Asofiei, Petre Chipurici

Factorial Design for Optimization of Microwave Assisted Synthesis of 5-Hydroxymethylfurfural

Abstract:

Synthesis of 5-hydroxymethylfurfural (5-HMF) by microwave assisted dehydration of fructose was performed under various operating conditions. A statistical analysis based on a 23 factorial plan was used to optimize the synthesis process. Operating temperature (110, 130 °C), specific mass of HCl catalyst (0.4, 0.6 mg/mgs), and reaction time (8, 12 min) were selected as process factors. A regression equation linking the process performance expressed as 5-HMF yield (7.40-30.60%) to process factors was established. The statistical model emphasized a better performance for higher levels of all process factors.
Keywords:
5-hydroxymethylfurfural; fructose; microwave assisted synthesis; design of experiments; acid catalyst

Issue: 2017, Volume 68, Issue 4
Pages: 639-641
Publication date: 2017/5/15
https://doi.org/10.37358/RC.17.4.5521
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Creative Commons License
This article is published under the Creative Commons Attribution 4.0 International License
Citation Styles
Cite this article as:
GAVRILA, A.I., ASOFIEI, I., CHIPURICI, P., Factorial Design for Optimization of Microwave Assisted Synthesis of 5-Hydroxymethylfurfural, Rev. Chim., 68(4), 2017, 639-641.

Vancouver
Gavrila AI, Asofiei I, Chipurici P. Factorial Design for Optimization of Microwave Assisted Synthesis of 5-Hydroxymethylfurfural. Rev. Chim.[internet]. 2017 Apr;68(4):639-641. Available from: https://doi.org/10.37358/RC.17.4.5521


APA 6th edition
Gavrila, A.I., Asofiei, I. & Chipurici, P. (2017). Factorial Design for Optimization of Microwave Assisted Synthesis of 5-Hydroxymethylfurfural. Revista de Chimie, 68(4), 639-641. https://doi.org/10.37358/RC.17.4.5521


Harvard
Gavrila, A.I., Asofiei, I., Chipurici, P. (2017). 'Factorial Design for Optimization of Microwave Assisted Synthesis of 5-Hydroxymethylfurfural', Revista de Chimie, 68(4), pp. 639-641. https://doi.org/10.37358/RC.17.4.5521


IEEE
A.I. Gavrila, I. Asofiei, P. Chipurici, "Factorial Design for Optimization of Microwave Assisted Synthesis of 5-Hydroxymethylfurfural". Revista de Chimie, vol. 68, no. 4, pp. 639-641, 2017. [online]. https://doi.org/10.37358/RC.17.4.5521


Text
Adina Ionuta Gavrila, Ioana Asofiei, Petre Chipurici,
Factorial Design for Optimization of Microwave Assisted Synthesis of 5-Hydroxymethylfurfural,
Revista de Chimie,
Volume 68, Issue 4,
2017,
Pages 639-641,
ISSN 2668-8212,
https://doi.org/10.37358/RC.17.4.5521.
(https://revistadechimie.ro/Articles.asp?ID=5521)
Keywords: 5-hydroxymethylfurfural; fructose; microwave assisted synthesis; design of experiments; acid catalyst


RIS
TY - JOUR
T1 - Factorial Design for Optimization of Microwave Assisted Synthesis of 5-Hydroxymethylfurfural
A1 - Gavrila, Adina Ionuta
A2 - Asofiei, Ioana
A3 - Chipurici, Petre
JF - Revista de Chimie
JO - Rev. Chim.
PB - Revista de Chimie SRL
SN - 2668-8212
Y1 - 2017
VL - 68
IS - 4
SP - 639
EP - 641
UR - https://doi.org/10.37358/RC.17.4.5521
KW - 5-hydroxymethylfurfural
KW - fructose
KW - microwave assisted synthesis
KW - design of experiments
KW - acid catalyst
ER -


BibTex
@article{RevCh2017P639,
author = {Gavrila Adina Ionuta and Asofiei Ioana and Chipurici Petre},
title = {Factorial Design for Optimization of Microwave Assisted Synthesis of 5-Hydroxymethylfurfural},
journal = {Revista de Chimie},
volume = {68},
number = {4},
pages = {639-641},
year = {2017},
issn = {2668-8212},
doi = {https://doi.org/10.37358/RC.17.4.5521},
url = {https://revistadechimie.ro/Articles.asp?ID=5521}
}
 
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