Study of Cotton Grafting with Hemiacetal - MCT-b-CD Derivative Using Fourier Transform Infrared Spectroscopy and Statistical Analysis

Popescu, Vasilica; Sandu, Irina Crina Anca; Popescu, Gabriel

Vasilica Popescu, Irina Crina Anca Sandu, Gabriel Popescu

Study of Cotton Grafting with Hemiacetal - MCT-b-CD Derivative Using Fourier Transform Infrared Spectroscopy and Statistical Analysis

Abstract:

The dihydrated forms of the 40% glyoxal solution undergo a dehydration process (in the presence of HCl), when the proportion of non-hydrated glyoxal increases. In the presence of a dilute ethanol solution, the non-hydrated glyoxal generates a hemiacetal. The presence of hemiacetal is confirmed by FT-IR analysis by increasing of the peaks at 1053 cm-1, 1107 cm-1 and by decreasing of the peak at 1746 cm-1. The grafting of cotton with the final grafting agent obtained from the interaction of hemiacetal with MCT-b-CD, was possible using pad-dry-cure technology. The presence of MCT-b-CD on cotton fabric was confirmed by FT-IR analysis (by the peaks of 1535 cm-1 and 787 cm-1) and by the yellowing of the sample. Confirmation of the grafting is given both by increasing the pickup / take-up degrees and by increasing the wrinkle recovery angles (WRA). The statistical analysis of these indices indicates low values for standard deviation (SD), standard error of the mean (SEM) and the coefficient of variation (CV).

Keywords:
grafting; hemiacetal; MCT-b-CD; FT-IR; statistical analysis

Issue: 2017, Volume 68, Issue 9

Pages: 2055-2059

Publication date: 2017/10/15

https://doi.org/10.37358/RC.17.9.5821

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This article is published under the Creative Commons Attribution 4.0 International License

Citation Styles

Cite this article as:
POPESCU, V., SANDU, I.C.A., POPESCU, G., Study of Cotton Grafting with Hemiacetal - MCT-b-CD Derivative Using Fourier Transform Infrared Spectroscopy and Statistical Analysis, Rev. Chim., 68(9), 2017, 2055-2059.

Vancouver
Popescu V, Sandu ICA, Popescu G. Study of Cotton Grafting with Hemiacetal - MCT-b-CD Derivative Using Fourier Transform Infrared Spectroscopy and Statistical Analysis. Rev. Chim.[internet]. 2017 Sep;68(9):2055-2059. Available from: https://doi.org/10.37358/RC.17.9.5821

APA 6th edition
Popescu, V., Sandu, I.C.A. & Popescu, G. (2017). Study of Cotton Grafting with Hemiacetal - MCT-b-CD Derivative Using Fourier Transform Infrared Spectroscopy and Statistical Analysis. Revista de Chimie, 68(9), 2055-2059. https://doi.org/10.37358/RC.17.9.5821

Harvard
Popescu, V., Sandu, I.C.A., Popescu, G. (2017). 'Study of Cotton Grafting with Hemiacetal - MCT-b-CD Derivative Using Fourier Transform Infrared Spectroscopy and Statistical Analysis', Revista de Chimie, 68(9), pp. 2055-2059. https://doi.org/10.37358/RC.17.9.5821

IEEE
V. Popescu, I.C.A. Sandu, G. Popescu, "Study of Cotton Grafting with Hemiacetal - MCT-b-CD Derivative Using Fourier Transform Infrared Spectroscopy and Statistical Analysis". Revista de Chimie, vol. 68, no. 9, pp. 2055-2059, 2017. [online]. https://doi.org/10.37358/RC.17.9.5821

Text
Vasilica Popescu, Irina Crina Anca Sandu, Gabriel Popescu,
Study of Cotton Grafting with Hemiacetal - MCT-b-CD Derivative Using Fourier Transform Infrared Spectroscopy and Statistical Analysis,
Revista de Chimie,
Volume 68, Issue 9,
2017,
Pages 2055-2059,
ISSN 2668-8212,
https://doi.org/10.37358/RC.17.9.5821.
(https://revistadechimie.ro/Articles.asp?ID=5821)
Keywords: grafting; hemiacetal; MCT-b-CD; FT-IR; statistical analysis

RIS
TY - JOUR
T1 - Study of Cotton Grafting with Hemiacetal - MCT-b-CD Derivative Using Fourier Transform Infrared Spectroscopy and Statistical Analysis
A1 - Popescu, Vasilica
A2 - Sandu, Irina Crina Anca
A3 - Popescu, Gabriel
JF - Revista de Chimie
JO - Rev. Chim.
PB - Revista de Chimie SRL
SN - 2668-8212
Y1 - 2017
VL - 68
IS - 9
SP - 2055
EP - 2059
UR - https://doi.org/10.37358/RC.17.9.5821
KW - grafting
KW - hemiacetal
KW - MCT-b-CD
KW - FT-IR
KW - statistical analysis
ER -

BibTex
@article{RevCh2017P2055,
author = {Popescu Vasilica and Sandu Irina Crina Anca and Popescu Gabriel},
title = {Study of Cotton Grafting with Hemiacetal - MCT-b-CD Derivative Using Fourier Transform Infrared Spectroscopy and Statistical Analysis},
journal = {Revista de Chimie},
volume = {68},
number = {9},
pages = {2055-2059},
year = {2017},
issn = {2668-8212},
doi = {https://doi.org/10.37358/RC.17.9.5821},
url = {https://revistadechimie.ro/Articles.asp?ID=5821}
}

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