Influence of Synthesis Parameters of FeNi3 Alloy Nanoparticles Obtained by Chemical Reduction Method in Aqueous Solution

Malaeru, Teodora; Patroi, Eros Alexandru; Patroi, Delia; Manta, Eugen; Marinescu, Virgil; Georgescu, Gabriela

Teodora Malaeru, Eros Alexandru Patroi, Delia Patroi, Eugen Manta, Virgil Marinescu, Gabriela Georgescu

Influence of Synthesis Parameters of FeNi3 Alloy Nanoparticles Obtained by Chemical Reduction Method in Aqueous Solution

Abstract:

This paper reports the synthesis of FeNi3 alloy nanoparticles by chemical reduction of the Fe2+ and Ni2+ ions, from the corresponding chlorides, with hydrazine (N2H4·H2O) as a reducing agent in aqueous solution at room temperature by modifying the molar ratio of the ions Fe2+: Ni2+, reaction time, with and without amine-type growth promoter, and reducing both, with or without ultrasonic aid. The FeNi3 alloy nanoparticles have been investigated by XRD, EDS spectrum analysis, SEM and VSM. When the molar ratio of Fe2+ and Ni2+ is equal to 1:3, reducing both, with or without ultrasonic aid, Fe2+ and Ni2+ were completely reduced into Fe and Ni, resulting FeNi3 alloy with a face-centered cubic (fcc) crystal structure. EDS analysis supported the presence of metal ions in atomic weight corresponding to the stoichiometric ratio of initial reaction. SEM analysis showed that nanoparticles of FeNi3 alloy have a spherical structural morphology. Hysteresis loop show a ferromagnetic behaviour of the FeNi3 alloy nanoparticles at room temperature.

Keywords:
FeNi3 alloy; reduction method; magnetic properties; saturation magnetization

Issue: 2019, Volume 70, Issue 4

Pages: 1118-1124

Publication date: 2019/5/15

https://doi.org/10.37358/RC.19.4.7076

Download Pdf Article

This article is published under the Creative Commons Attribution 4.0 International License

Citation Styles

Cite this article as:
MALAERU, T., PATROI, E.A., PATROI, D., MANTA, E., MARINESCU, V., GEORGESCU, G., Influence of Synthesis Parameters of FeNi3 Alloy Nanoparticles Obtained by Chemical Reduction Method in Aqueous Solution, Rev. Chim., 70(4), 2019, 1118-1124.

Vancouver
Malaeru T, Patroi EA, Patroi D, Manta E, Marinescu V, Georgescu G. Influence of Synthesis Parameters of FeNi3 Alloy Nanoparticles Obtained by Chemical Reduction Method in Aqueous Solution. Rev. Chim.[internet]. 2019 Apr;70(4):1118-1124. Available from: https://doi.org/10.37358/RC.19.4.7076

APA 6th edition
Malaeru, T., Patroi, E.A., Patroi, D., Manta, E., Marinescu, V. & Georgescu, G. (2019). Influence of Synthesis Parameters of FeNi3 Alloy Nanoparticles Obtained by Chemical Reduction Method in Aqueous Solution. Revista de Chimie, 70(4), 1118-1124. https://doi.org/10.37358/RC.19.4.7076

Harvard
Malaeru, T., Patroi, E.A., Patroi, D., Manta, E., Marinescu, V., Georgescu, G. (2019). 'Influence of Synthesis Parameters of FeNi3 Alloy Nanoparticles Obtained by Chemical Reduction Method in Aqueous Solution', Revista de Chimie, 70(4), pp. 1118-1124. https://doi.org/10.37358/RC.19.4.7076

IEEE
T. Malaeru, E.A. Patroi, D. Patroi, E. Manta, V. Marinescu, G. Georgescu, "Influence of Synthesis Parameters of FeNi3 Alloy Nanoparticles Obtained by Chemical Reduction Method in Aqueous Solution". Revista de Chimie, vol. 70, no. 4, pp. 1118-1124, 2019. [online]. https://doi.org/10.37358/RC.19.4.7076

Text
Teodora Malaeru, Eros Alexandru Patroi, Delia Patroi, Eugen Manta, Virgil Marinescu, Gabriela Georgescu,
Influence of Synthesis Parameters of FeNi3 Alloy Nanoparticles Obtained by Chemical Reduction Method in Aqueous Solution,
Revista de Chimie,
Volume 70, Issue 4,
2019,
Pages 1118-1124,
ISSN 2668-8212,
https://doi.org/10.37358/RC.19.4.7076.
(https://revistadechimie.ro/Articles.asp?ID=7076)
Keywords: FeNi3 alloy; reduction method; magnetic properties; saturation magnetization

RIS
TY - JOUR
T1 - Influence of Synthesis Parameters of FeNi3 Alloy Nanoparticles Obtained by Chemical Reduction Method in Aqueous Solution
A1 - Malaeru, Teodora
A2 - Patroi, Eros Alexandru
A3 - Patroi, Delia
A4 - Manta, Eugen
A5 - Marinescu, Virgil
A6 - Georgescu, Gabriela
JF - Revista de Chimie
JO - Rev. Chim.
PB - Revista de Chimie SRL
SN - 2668-8212
Y1 - 2019
VL - 70
IS - 4
SP - 1118
EP - 1124
UR - https://doi.org/10.37358/RC.19.4.7076
KW - FeNi3 alloy
KW - reduction method
KW - magnetic properties
KW - saturation magnetization
ER -

BibTex
@article{RevCh2019P1118,
author = {Malaeru Teodora and Patroi Eros Alexandru and Patroi Delia and Manta Eugen and Marinescu Virgil and Georgescu Gabriela},
title = {Influence of Synthesis Parameters of FeNi3 Alloy Nanoparticles Obtained by Chemical Reduction Method in Aqueous Solution},
journal = {Revista de Chimie},
volume = {70},
number = {4},
pages = {1118-1124},
year = {2019},
issn = {2668-8212},
doi = {https://doi.org/10.37358/RC.19.4.7076},
url = {https://revistadechimie.ro/Articles.asp?ID=7076}
}

<<<< back

PUBLISHING SECTION

Author Guidelines

* Paper Drafting

* Paper Template

* Ethical Statement

* Paper Submission

Ghidul Autorului (ro)

Open Access & Archiving Policy

Search Authors

LATEST NEWS
	NUMAR OMAGIAL PETRU PONI.. detalii
	Revista de Chimie - 70 de ani de aparitie neintrerupta.. detalii
	English-Romanian Dictionary for Mechanical Engineering (download pdf)