Validation and Quality Assurance of Ascorbic Acid Determination in Agricultural Products

Hegedus, Ondrej; Szarka, Katarina; Hegedusova, Alzbeta; Godany, Zsuzsanna; Slosar, Miroslav; Nechifor, Aurelia Cristina; Tonk, Szende

Ondrej Hegedus, Katarina Szarka, Alzbeta Hegedusova, Zsuzsanna Godany, Miroslav Slosar, Aurelia Cristina Nechifor, Szende Tonk

Validation and Quality Assurance of Ascorbic Acid Determination in Agricultural Products

Abstract:

The study describes a method for the determination of ascorbic acid (AA) with the technique of high performance liquid chromatography with UV detection (UV-HPLC) modified for routine analysis of agricultural products. For successful use of the method in the test laboratory practice, the reliability of using this method has been confirmed by validation. The repeatability of method has been observed, which is 2.80 - 5.55% for the various crops. Relative combined standard uncertainty has a value of 6.2%. The accuracy of the method is 103.2% and calculated as recovery of the standard addition. The value of the LOQ computed from the upper limit of reliability is 26.7 mg kg-1, which ensures safe determination of AA in every major agricultural crop.

Keywords:
ascorbic acid; agricultural products; determination; method validation; quality assurance

Issue: 2019, Volume 70, Issue 7

Pages: 2308-2314

Publication date: 2019/8/15

https://doi.org/10.37358/RC.19.7.7329

Download Pdf Article

This article is published under the Creative Commons Attribution 4.0 International License

Citation Styles

Cite this article as:
HEGEDUS, O., SZARKA, K., HEGEDUSOVA, A., GODANY, Z., SLOSAR, M., NECHIFOR, A.C., TONK, S., Validation and Quality Assurance of Ascorbic Acid Determination in Agricultural Products, Rev. Chim., 70(7), 2019, 2308-2314.

Vancouver
Hegedus O, Szarka K, Hegedusova A, Godany Z, Slosar M, Nechifor AC, Tonk S. Validation and Quality Assurance of Ascorbic Acid Determination in Agricultural Products. Rev. Chim.[internet]. 2019 Jul;70(7):2308-2314. Available from: https://doi.org/10.37358/RC.19.7.7329

APA 6th edition
Hegedus, O., Szarka, K., Hegedusova, A., Godany, Z., Slosar, M., Nechifor, A.C. & Tonk, S. (2019). Validation and Quality Assurance of Ascorbic Acid Determination in Agricultural Products. Revista de Chimie, 70(7), 2308-2314. https://doi.org/10.37358/RC.19.7.7329

Harvard
Hegedus, O., Szarka, K., Hegedusova, A., Godany, Z., Slosar, M., Nechifor, A.C., Tonk, S. (2019). 'Validation and Quality Assurance of Ascorbic Acid Determination in Agricultural Products', Revista de Chimie, 70(7), pp. 2308-2314. https://doi.org/10.37358/RC.19.7.7329

IEEE
O. Hegedus, K. Szarka, A. Hegedusova, Z. Godany, M. Slosar, A.C. Nechifor, S. Tonk, "Validation and Quality Assurance of Ascorbic Acid Determination in Agricultural Products". Revista de Chimie, vol. 70, no. 7, pp. 2308-2314, 2019. [online]. https://doi.org/10.37358/RC.19.7.7329

Text
Ondrej Hegedus, Katarina Szarka, Alzbeta Hegedusova, Zsuzsanna Godany, Miroslav Slosar, Aurelia Cristina Nechifor, Szende Tonk,
Validation and Quality Assurance of Ascorbic Acid Determination in Agricultural Products,
Revista de Chimie,
Volume 70, Issue 7,
2019,
Pages 2308-2314,
ISSN 2668-8212,
https://doi.org/10.37358/RC.19.7.7329.
(https://revistadechimie.ro/Articles.asp?ID=7329)
Keywords: ascorbic acid; agricultural products; determination; method validation; quality assurance

RIS
TY - JOUR
T1 - Validation and Quality Assurance of Ascorbic Acid Determination in Agricultural Products
A1 - Hegedus, Ondrej
A2 - Szarka, Katarina
A3 - Hegedusova, Alzbeta
A4 - Godany, Zsuzsanna
A5 - Slosar, Miroslav
A6 - Nechifor, Aurelia Cristina
A7 - Tonk, Szende
JF - Revista de Chimie
JO - Rev. Chim.
PB - Revista de Chimie SRL
SN - 2668-8212
Y1 - 2019
VL - 70
IS - 7
SP - 2308
EP - 2314
UR - https://doi.org/10.37358/RC.19.7.7329
KW - ascorbic acid
KW - agricultural products
KW - determination
KW - method validation
KW - quality assurance
ER -

BibTex
@article{RevCh2019P2308,
author = {Hegedus Ondrej and Szarka Katarina and Hegedusova Alzbeta and Godany Zsuzsanna and Slosar Miroslav and Nechifor Aurelia Cristina and Tonk Szende},
title = {Validation and Quality Assurance of Ascorbic Acid Determination in Agricultural Products},
journal = {Revista de Chimie},
volume = {70},
number = {7},
pages = {2308-2314},
year = {2019},
issn = {2668-8212},
doi = {https://doi.org/10.37358/RC.19.7.7329},
url = {https://revistadechimie.ro/Articles.asp?ID=7329}
}

<<<< back

PUBLISHING SECTION

Author Guidelines

* Paper Drafting

* Paper Template

* Ethical Statement

* Paper Submission

Ghidul Autorului (ro)

Open Access & Archiving Policy

Search Authors

LATEST NEWS
	NUMAR OMAGIAL PETRU PONI.. detalii
	Revista de Chimie - 70 de ani de aparitie neintrerupta.. detalii
	English-Romanian Dictionary for Mechanical Engineering (download pdf)