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REVISTA DE CHIMIE
Cite as: Rev. Chim.
https://doi.org/10.37358/Rev.Chim.1949

OSIM Nr. R102355
ISSN Online 2668-8212
ISSN Print: 1582-9049
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Revista de Chimie (Rev. Chim.), Year 2015, Volume 66, Issue 1,





LAURA GABRIELA SARBU, ION SANDU, LUCIAN GABRIEL BAHRIN, ADRIANA BALAN, MIRCEA ODIN APOSTU
New Bromo Substituted 1,3-Dithiol-2-ylium Salts

Abstract:

A series of 5-bromo-2-(N,N-dimethylamino)-1,3-dithiol-2-ylium compounds have been synthesized by the bromination of the corresponding 6-[2-(N,N-dimethylamino)-1,3-dithiol-2-ylium-4-yl]phenolates at the C(5) position of the 1,3-dithiol ring. The latter compounds have been obtained by heterocyclofunctionalization of some xylenols. The structure of 5-bromo-4-(3-bromo-4,5-dimethyl-2-hydroxyphenyl)-2-(N,N-dimethylamino)-1,3-dithiol-2-ylium bromide (7a) was unambigously proved by X-ray crystallography. Keywords: bromination, dithiocarbamates, 1,3-dithiolium salts, mesoionic compounds, X-ray crystallography

Issue: 2015, Volume 66, Issue 1
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