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https://doi.org/10.37358/Rev.Chim.1949

OSIM Nr. R102355
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Revista de Chimie (Rev. Chim.), Year 2019, Volume 70, Issue 11, 3921-3925

https://doi.org/10.37358/RC.70.19.11.7673

Monica Catana, Luminita Catana, Enuta Iorga, Adrian Constantin Asanica, Anda Gratiela Lazar, Monica Alexandra Lazar, Nastasia Belc, Gina Pirvu

Internal Validation of Rapid and Performance Method for Patulin Determination in Apple Cider by High-Performance Liquid Chromatography

Abstract:

An analytical method was developed and validated for separation, detection and quantification of patulin in apple cider by high-performance liquid chromatography (HPLC-DAD). Extraction and clean-up of patulin from apple cider are achieved on AFFINIMIP® SPE PATULIN cartridge (3mL/100mg). Patulin was separated on a C18 Hypersil GOLD column (150 mm × 4 mm, 5 mm) coupled to a Hypersil Gold guard column (10 × 4.0 mm, 5 mm) using mobile phase consisting of water:acetonitrile (95:5, v/v) and detected at 276 nm. The method has a good sensitivity (LOD = 2.63 mg/mL and LOQ = 8.45mg/mL) and a good precision (RDS (r) = 0.32...0.91% for injection repeatability; RSD (r) = 1.05….2.98% for analysis repeatability intra-day; RSD (R) = 1.35….3.24% for intermediate precision; RSD (R) = 1.64….3.86% for intra-laboratory reproducibility). The method was applied by analyzing samples of apple cider purchased from commerce. In case of 80% of the analyzed samples, patulin was not detected, and for the rest of them concentration of patulin was [ LOQ.
Keywords:
patulin; validation; HPLC-DAD; apple cider

Issue: 2019, Volume 70, Issue 11
Pages: 3921-3925
Publication date: 2019/12/15
https://doi.org/10.37358/RC.70.19.11.7673
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Creative Commons License
This article is published under the Creative Commons Attribution 4.0 International License
Citation Styles
Cite this article as:
CATANA, M., CATANA, L., IORGA, E., ASANICA, A.C., LAZAR, A.G., LAZAR, M.A., BELC, N., PIRVU, G., Internal Validation of Rapid and Performance Method for Patulin Determination in Apple Cider by High-Performance Liquid Chromatography, Rev. Chim., 70(11), 2019, 3921-3925.

Vancouver
Catana M, Catana L, Iorga E, Asanica AC, Lazar AG, Lazar MA, Belc N, Pirvu G. Internal Validation of Rapid and Performance Method for Patulin Determination in Apple Cider by High-Performance Liquid Chromatography. Rev. Chim.[internet]. 2019 Nov;70(11):3921-3925. Available from: https://doi.org/10.37358/RC.70.19.11.7673


APA 6th edition
Catana, M., Catana, L., Iorga, E., Asanica, A.C., Lazar, A.G., Lazar, M.A., Belc, N. & Pirvu, G. (2019). Internal Validation of Rapid and Performance Method for Patulin Determination in Apple Cider by High-Performance Liquid Chromatography. Revista de Chimie, 70(11), 3921-3925. https://doi.org/10.37358/RC.70.19.11.7673


Harvard
Catana, M., Catana, L., Iorga, E., Asanica, A.C., Lazar, A.G., Lazar, M.A., Belc, N., Pirvu, G. (2019). 'Internal Validation of Rapid and Performance Method for Patulin Determination in Apple Cider by High-Performance Liquid Chromatography', Revista de Chimie, 70(11), pp. 3921-3925. https://doi.org/10.37358/RC.70.19.11.7673


IEEE
M. Catana, L. Catana, E. Iorga, A.C. Asanica, A.G. Lazar, M.A. Lazar, N. Belc, G. Pirvu, "Internal Validation of Rapid and Performance Method for Patulin Determination in Apple Cider by High-Performance Liquid Chromatography". Revista de Chimie, vol. 70, no. 11, pp. 3921-3925, 2019. [online]. https://doi.org/10.37358/RC.70.19.11.7673


Text
Monica Catana, Luminita Catana, Enuta Iorga, Adrian Constantin Asanica, Anda Gratiela Lazar, Monica Alexandra Lazar, Nastasia Belc, Gina Pirvu,
Internal Validation of Rapid and Performance Method for Patulin Determination in Apple Cider by High-Performance Liquid Chromatography,
Revista de Chimie,
Volume 70, Issue 11,
2019,
Pages 3921-3925,
ISSN 2668-8212,
https://doi.org/10.37358/RC.70.19.11.7673.
(https://revistadechimie.ro/Articles.asp?ID=7673)
Keywords: patulin; validation; HPLC-DAD; apple cider


RIS
TY - JOUR
T1 - Internal Validation of Rapid and Performance Method for Patulin Determination in Apple Cider by High-Performance Liquid Chromatography
A1 - Catana, Monica
A2 - Catana, Luminita
A3 - Iorga, Enuta
A4 - Asanica, Adrian Constantin
A5 - Lazar, Anda Gratiela
A6 - Lazar, Monica Alexandra
A7 - Belc, Nastasia
A8 - Pirvu, Gina
JF - Revista de Chimie
JO - Rev. Chim.
PB - Revista de Chimie SRL
SN - 2668-8212
Y1 - 2019
VL - 70
IS - 11
SP - 3921
EP - 3925
UR - https://doi.org/10.37358/RC.70.19.11.7673
KW - patulin
KW - validation
KW - HPLC-DAD
KW - apple cider
ER -


BibTex
@article{RevCh2019P3921,
author = {Catana Monica and Catana Luminita and Iorga Enuta and Asanica Adrian Constantin and Lazar Anda Gratiela and Lazar Monica Alexandra and Belc Nastasia and Pirvu Gina},
title = {Internal Validation of Rapid and Performance Method for Patulin Determination in Apple Cider by High-Performance Liquid Chromatography},
journal = {Revista de Chimie},
volume = {70},
number = {11},
pages = {3921-3925},
year = {2019},
issn = {2668-8212},
doi = {https://doi.org/10.37358/RC.70.19.11.7673},
url = {https://revistadechimie.ro/Articles.asp?ID=7673}
}
 
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