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REVISTA DE CHIMIE
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https://doi.org/10.37358/Rev.Chim.1949

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Revista de Chimie (Rev. Chim.), Year 2008, Volume 59, Issue 1, 56-60

https://doi.org/10.37358/RC.08.1.1707

Ioana M.c. Ienascu, Alfa X. Lupea, Iuliana M. Popescu, Stefan Th. Tomas, Alina D. Zamfir

Synthesis and Characterization of Some New 2-Hydroxy-N-(3-Trifluoromethyl-Phenyl)-Benzamide Derivatives

Abstract:

In the reaction between 2-hydroxy-N-(3-trifluoromethyl-phenyl)-benzamide and chloro-acetic acid ethyl ester, [2-(3-trifluoromethyl-phenylcarbamoyl)-phenoxy]-acetic acid ethyl ester was obtained. The ethyl ester was condensed with hydrazine giving 2-hydrazinocarbonylmethoxy-N-(3-trifluoromethyl-phenyl)-benzamide. This hydrazide is considered the key intermediate for the synthesis of new compounds. So, in the reaction between hydrazide and chloro-substituted benzaldehydes hydrazones were obtained. In order to establish their structures, all new synthesized compounds were analyzed by modern physico-chemical methods (FTIR, 1H-NMR, 13C-NMR, MS).
Keywords:
2-hydroxy-N-(3-trifluoromethyl-phenyl)-benzamide derivatives; ethyl esters; hydrazides; hydrazones; salicylanilide-O-substituted

Issue: 2008, Volume 59, Issue 1
Pages: 56-60
Publication date: 09/02/2008
https://doi.org/10.37358/RC.08.1.1707
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This article is published under the Creative Commons Attribution 4.0 International License
 
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