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REVISTA DE CHIMIE
Cite as: Rev. Chim.
https://doi.org/10.37358/Rev.Chim.1949

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Revista de Chimie (Rev. Chim.), Year 2009, Volume 60, Issue 1,





Electrochemical Behaviour of Mo Ions in Alkali Halide Electrolytes

Abstract:

The electrochemical properties of solution of molybdenum ions in molten alkali halide electrolytes were studied at 1023-1123 K. The chemical and electrochemical stability of solutions is an important parameter, which must be controlled to ensure reproducible electrochemical measurements. Polarization and voltammetric curves at tungsten electrode revealed the existence of a reversible electrochemical process between the species Mo(III) and Mo(0) with a standard potential equal to 812 mV vs. Ag/AgCl reference electrode. The reduction process Mo(III) to Mo(0) appears as a single reversible three-electron exchange couple with significant crystallization problems. Keywords: molten salts, electrochemistry, molybdenum

Issue: 2009, Volume 60, Issue 1
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