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REVISTA DE CHIMIE
Cite as: Rev. Chim.
https://doi.org/10.37358/Rev.Chim.1949

OSIM Nr. R102355
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Revista de Chimie (Rev. Chim.), Year 2015, Volume 66, Issue 1,





MIRCEA ODIN APOSTU, IOAN GABRIEL SANDU, LUCIAN MIHAIL BIRSA, KAMEL EARAR
Synthesis of Novel 4-Aryl-5-Methyl-1,3-Dithiolium Derivatives

Abstract:

Novel 4,6-dibromo-2-[5-methyl-2-(N,N-dialkylamino)-1,3-dithiol-2-ylium-4-yl]phenolates have been synthesized by the heterocondensation of the 1-(3,5-dibromo-2-hydroxyphenyl)-1-oxapropan-2-yl dithiocarbamates. The latter compounds have been obtained from the reaction of the corresponding substituted a-bromopropiophenone with various salts of dithiocarbamic acids. The structure of 1-(3,5-dibromo-2-hydroxyphenyl)-1-oxapropan-2-yl-piperidine-1-carbodithioate (2b) was unambigously proved by X-ray crystallography. Keywords: dithiocarbamates, 1,3-dithiolium salts,mesoionic compounds, propiophenones, X-ray crystallography

Issue: 2015, Volume 66, Issue 1
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