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Revista de Chimie (Rev. Chim.), Year 2016, Volume 67, Issue 1,



Laura-Ileana Socea, Gabriel Saramet, Constantin Draghici, Stefania-Felicia Barbuceanu, Diana Carolina Ilies, Bogdan Socea

Research on the Synthesis and Characterization of New 1,3,4-oxadiazoles with 5H-dibenzo<7>annulene Moiety

Abstract:

A series of 2-amino-1,3,4-oxadiazoles 4a-f with 5H-dibenzo<7>annulene moiety were synthesized by cyclization of 2- acylhydrazinecarbothioamides 3a-f in the presence of mercury oxide. 2-Acylhidrazinecarbothioamide 3a-f were synthesized by nucleophilic addition of 2-(5H-dibenzo<7>annulen-5-yl)acetohydrazide to different isothiocyanates. All the newly synthesized compounds were characterized by their spectral data (IR, 1H-NMR and 13C-NMR spectroscopy) and elemental analysis.
Keywords:
5H-dibenzo<7>annulene; 2-amino-1;3;4-oxadiazole; hydrazinecarbothioamide

Issue: 2016, Volume 67, Issue 1
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