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REVISTA DE CHIMIE
Cite as: Rev. Chim.
https://doi.org/10.37358/Rev.Chim.1949

OSIM Nr. R102355
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Revista de Chimie (Rev. Chim.), Year 2016, Volume 67, Issue 1,



Lucian Gabriel Bahrin, Henning Hopf, Peter George Jones, Kamel Earar, Lucian Mihail Birsa

Synthesis and Structural Characterization of a New Iodine-containing Phenacyl N,N-Diethylamino Carbodithioate

Abstract:

The synthesis of 1-(2-hydroxy-5-iodophenyl)-1-oxaethan-2-yl-N,N-diethylamino-1-carbodithioate was achieved from w-bromo-2-hydroxy-5-iodoacetophenone and sodium N,N-diethyldithiocarbamate, and the structure of the new phenacyl carbodithioate was confirmed by X-ray analysis. Upon acid-catalyzed cyclization of dithiocarbamate 3, the corresponding 1,3-dithiolium perchlorate 4 was obtained. Conversion of the latter into mesoionic derivative 5 was achieved in a basic environment. All new compounds were characterized using NMR spectroscopy.
Keywords:
dithiocarbamate; 1;3-dithiolium salt; mesoionic phenolate; X-ray crystallography

Issue: 2016, Volume 67, Issue 1
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