Novel Multiresidue Method for the Determination of Eight Trichothecene Mycotoxins in Pollen Samples Using QuEChERS-Based GC-MS/MS

Morariu, Ionela Daniela; Avasilcai, Liliana; Vieriu, Madalina; Panainte, Alina Diana; Bibire, Nela

Ionela Daniela Morariu, Liliana Avasilcai, Madalina Vieriu, Alina Diana Panainte, Nela Bibire

Novel Multiresidue Method for the Determination of Eight Trichothecene Mycotoxins in Pollen Samples Using QuEChERS-Based GC-MS/MS

Abstract:

A simple multi-residue method based on QuEChERS-sample preparation was developed for the determination of eight trichothecene mycotoxins (nivalenol, fusarenon-x, diacetoxyscirpenol, 3-acetyl-deoxynivalenol, neosolaniol, deoxynivalenol, T-2 and HT-2 toxins) in pollen, using gas chromatography coupled with mass spectrometry. The developed method was validated by evaluating the following parameters: linearity, limit of quantification, matrix effect and precision of measurements. All mycotoxins showed good linearity. The method gave good recoveries (91-104%) with RSDs ] 11% for most of the analites (6 out of 8). The limits of quantification varied from 1 to 4µg·kg--1.

Keywords:
mycotoxins; bee pollen; GS-MS/MS; QuEChERS; triple quadrupole

Issue: 2017, Volume 68, Issue 2

Pages: 304-306

Publication date: 2017/3/15

https://doi.org/10.37358/RC.17.2.5441

Download Pdf Article

This article is published under the Creative Commons Attribution 4.0 International License

Citation Styles

Cite this article as:
MORARIU, I.D., AVASILCAI, L., VIERIU, M., PANAINTE, A.D., BIBIRE, N., Novel Multiresidue Method for the Determination of Eight Trichothecene Mycotoxins in Pollen Samples Using QuEChERS-Based GC-MS/MS, Rev. Chim., 68(2), 2017, 304-306.

Vancouver
Morariu ID, Avasilcai L, Vieriu M, Panainte AD, Bibire N. Novel Multiresidue Method for the Determination of Eight Trichothecene Mycotoxins in Pollen Samples Using QuEChERS-Based GC-MS/MS. Rev. Chim.[internet]. 2017 Feb;68(2):304-306. Available from: https://doi.org/10.37358/RC.17.2.5441

APA 6th edition
Morariu, I.D., Avasilcai, L., Vieriu, M., Panainte, A.D. & Bibire, N. (2017). Novel Multiresidue Method for the Determination of Eight Trichothecene Mycotoxins in Pollen Samples Using QuEChERS-Based GC-MS/MS. Revista de Chimie, 68(2), 304-306. https://doi.org/10.37358/RC.17.2.5441

Harvard
Morariu, I.D., Avasilcai, L., Vieriu, M., Panainte, A.D., Bibire, N. (2017). 'Novel Multiresidue Method for the Determination of Eight Trichothecene Mycotoxins in Pollen Samples Using QuEChERS-Based GC-MS/MS', Revista de Chimie, 68(2), pp. 304-306. https://doi.org/10.37358/RC.17.2.5441

IEEE
I.D. Morariu, L. Avasilcai, M. Vieriu, A.D. Panainte, N. Bibire, "Novel Multiresidue Method for the Determination of Eight Trichothecene Mycotoxins in Pollen Samples Using QuEChERS-Based GC-MS/MS". Revista de Chimie, vol. 68, no. 2, pp. 304-306, 2017. [online]. https://doi.org/10.37358/RC.17.2.5441

Text
Ionela Daniela Morariu, Liliana Avasilcai, Madalina Vieriu, Alina Diana Panainte, Nela Bibire,
Novel Multiresidue Method for the Determination of Eight Trichothecene Mycotoxins in Pollen Samples Using QuEChERS-Based GC-MS/MS,
Revista de Chimie,
Volume 68, Issue 2,
2017,
Pages 304-306,
ISSN 2668-8212,
https://doi.org/10.37358/RC.17.2.5441.
(https://revistadechimie.ro/Articles.asp?ID=5441)
Keywords: mycotoxins; bee pollen; GS-MS/MS; QuEChERS; triple quadrupole

RIS
TY - JOUR
T1 - Novel Multiresidue Method for the Determination of Eight Trichothecene Mycotoxins in Pollen Samples Using QuEChERS-Based GC-MS/MS
A1 - Morariu, Ionela Daniela
A2 - Avasilcai, Liliana
A3 - Vieriu, Madalina
A4 - Panainte, Alina Diana
A5 - Bibire, Nela
JF - Revista de Chimie
JO - Rev. Chim.
PB - Revista de Chimie SRL
SN - 2668-8212
Y1 - 2017
VL - 68
IS - 2
SP - 304
EP - 306
UR - https://doi.org/10.37358/RC.17.2.5441
KW - mycotoxins
KW - bee pollen
KW - GS-MS/MS
KW - QuEChERS
KW - triple quadrupole
ER -

BibTex
@article{RevCh2017P304,
author = {Morariu Ionela Daniela and Avasilcai Liliana and Vieriu Madalina and Panainte Alina Diana and Bibire Nela},
title = {Novel Multiresidue Method for the Determination of Eight Trichothecene Mycotoxins in Pollen Samples Using QuEChERS-Based GC-MS/MS},
journal = {Revista de Chimie},
volume = {68},
number = {2},
pages = {304-306},
year = {2017},
issn = {2668-8212},
doi = {https://doi.org/10.37358/RC.17.2.5441},
url = {https://revistadechimie.ro/Articles.asp?ID=5441}
}

<<<< back

PUBLISHING SECTION

Author Guidelines

* Paper Drafting

* Paper Template

* Ethical Statement

* Paper Submission

Ghidul Autorului (ro)

Open Access & Archiving Policy

Search Authors

LATEST NEWS
	NUMAR OMAGIAL PETRU PONI.. detalii
	Revista de Chimie - 70 de ani de aparitie neintrerupta.. detalii
	English-Romanian Dictionary for Mechanical Engineering (download pdf)